Question

What are the physicochemical technical parameters of papermaking defoamer XS-02, polyether ester defoamer?

Answer

Papermaking defoamer XS-02 is a nonionic polyether ester defoamer with polyoxyethylene oleate as the main component. Its main physicochemical parameters include appearance, pH, density, viscosity, HLB value, cloud point, flash point, and other indicators, overall performance is mild and stable.

Detailed Description

Papermaking defoamer XS-02 (CAS: 9004-81-3) appears as a milky white to light yellow viscous liquid, with molecular structure C17H33COO(CH2CH2O)nH, molecular weight range approximately 400~1500. The product's active ingredient content (solid content) is ≥99%, moisture content ≤0.5%, free alcohol content ≤1.0%, and it is a high-purity defoamer product.

The HLB value of this product is between 4 and 8, belonging to the water-in-oil (W/O) emulsifier category, with a low cloud point (15~30°C), and it is easy to self-emulsify and disperse in water. Its acid value ≤3.0 mgKOH/g, saponification value 40~140 mgKOH/g, hydroxyl value 45~60 mgKOH/g, iodine value 20~60 gI₂/100g, indicating moderate unsaturation, and the ester bond structure may undergo hydrolysis under strong alkaline conditions, which should be considered in formulation design.

In terms of safety performance, the product has a flash point (closed cup) >150°C, belongs to non-flammable liquid, non-explosive and non-oxidizing. The pH value of 1% and 5% aqueous solutions are both 5.0~8.0, close to neutral, non-irritating to skin and eyes, acute oral toxicity LD50 >2000 mg/kg, belongs to low-toxicity substance, with good environmental compatibility.

Technical Parameters

Parameter Name Indicator Range / Description Parameter Name Indicator Range / Description
Product NamePolyoxyethylene MonooleateIonic TypeNonionic
CAS Number9004-81-3Appearance (25°C)Milky white to light yellow viscous liquid
Molecular FormulaC17H33COO(CH2CH2O)nHMolecular WeightApproximately 400~1500
Active Ingredient / Solid Content≥99%Moisture≤0.5%
Density (25°C)0.85~1.05 g/cm³Kinematic Viscosity (25°C)100~500 mPa·s
Low Shear Viscosity100~500 mPa·sRefractive Index1.45~1.47
HLB Value4~8Cloud Point15~30°C
pH (1% Aqueous Solution)5.0~8.0pH (5% Aqueous Solution)5.0~8.0
Acid Value≤3.0 mgKOH/gSaponification Value40~140 mgKOH/g
Hydroxyl Value45~60 mgKOH/gIodine Value20~60 gI₂/100g
Surface TensionApproximately 25~30 mN/mCritical Micelle Concentration (CMC)10~100 mg/L
Flash Point (Closed Cup)>150°CFreezing Point / Melting Point<-10°C (liquid at room temperature)
Water SolubilityEasily dispersible in water (self-emulsifying)Foam CharacteristicsLow foam, defoaming function
Free Alcohol Content≤1.0%Heavy Metals (as Pb)≤20 mg/kg
Arsenic (As)≤2 mg/kgHygroscopicitySlightly hygroscopic
Chemical StabilityStable under normal conditionsAlkali ResistanceGeneral, ester bond may hydrolyze under strong base
UnsaturationModeratePackaging Specifications50kg plastic drum / 200kg plastic drum / IBC tote

Application Recommendations

Based on its HLB value (4~8) and cloud point (15~30°C) characteristics, this product is particularly suitable for medium to high temperature conditions in the paper industry. Recommended addition amounts vary by process: for black liquor defoaming, it is recommended to add 0.01%~0.1% of the total system mass; for paper machine white water circulation systems, recommended addition of 0.005%~0.05%; for coating defoaming, recommended addition of 0.1%~0.3%. Due to its nonionic nature, it is compatible with anionic, cationic auxiliaries, and sizing agents, without causing precipitation or side reactions.

It is worth noting that the ester bond structure of the product may undergo hydrolysis under strong alkaline conditions (pH>12) at high temperatures, leading to gradual degradation of defoaming performance. In alkaline pulping black liquor applications, continuous drip feeding is recommended to maintain stable defoaming and foam suppression effects. Additionally, the low cloud point (15~30°C) means that the product may precipitate or have reduced dispersibility in low-temperature water systems. In winter, ensure the system temperature is above the cloud point, or pre-disperse with warm water before addition.

Precautions

  • Storage Temperature: Store in a cool, dry place at 5~35°C, sealed, avoid low-temperature freezing and high-temperature exposure.
  • Operation Protection: Although it is a low-toxicity non-hazardous substance, it is recommended to wear protective gloves and goggles during handling, and wash hands thoroughly after operation.
  • Compatibility Testing: Before compounding with other auxiliaries, it is recommended to perform a small-scale compatibility test to confirm no adverse reactions before batch application.
  • Wastewater Treatment: The product is readily biodegradable, but spills should not be discharged directly into sewers or surface waters; collect and dispose of according to local regulations.